Ultrasonic assisted synthesis of imidazo[1,2-a]azine catalyzed by ZnO nanorods
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چکیده
منابع مشابه
Microwave Assisted Synthesis of N-Benzylenaminones Catalyzed by Chloroacetic acid
Benzylaminoalkenones and benzylaminoalkenoates 3 were synthesized from reaction of benzylamine with corresponding 1,3-diketones and 1,3-ketoesters in the presence of catalytic amount of chloroacetic acid under microwave radiation. This method offers several advantages including high yield of products, recyclable of the catalyst and easy experimental work-up procedure.
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Beside longitudinal growth along the length, we show that ZnO nanorods also exhibit transverse growth, which is responsible for the formation of interpenetrative nanorods. The longitudinal growth is lead by the catalytically active Zn-terminated (0001) surface, while the oxygen-terminated ð000 1Þ surface is catalytically inactive, resulting in the formation of ‘pencil’ or ‘bullet’ shaped nanost...
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ZnO nanorod was prepared by microwave assisted method. The crystal structure of the nano powders were confirmed by X-Ray diffraction analysis and the mean particle size was estimated by the Scherrer,s formula .The surface morphology of the nano particles were analyzed by using SEM . The absorption spectrum of the material in the UV-Vis range was recorded .The energy band gap of the...
متن کاملStructural, optical and dielectric studies in ZnO nanorods by microwave assisted method
ZnO nanorod was prepared by microwave assisted method. The crystal structure of the nano powders were confirmed by X-Ray diffraction analysis and the mean particle size was estimated by the Scherrer,s formula .The surface morphology of the nano particles were analyzed by using SEM . The absorption spectrum of the material in the UV-Vis range was recorded .The energy band gap of the...
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BACKGROUND Most of the known approaches to the synthesis of CF3-containing organic compounds suffer from serious drawbacks. For example the starting materials required for these methods are rather difficult to obtain, or they are fairly toxic and inconvenient to work with and methods for direct fluorination and trifluoromethylation do not always allow the introduction of the CF3-group at the re...
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ژورنال
عنوان ژورنال: Ultrasonics Sonochemistry
سال: 2013
ISSN: 1350-4177
DOI: 10.1016/j.ultsonch.2012.09.006